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Organic Syntheses, Volume 71

ISBN: 978-0-471-30531-6
320 pages
August 1993
Organic Syntheses, Volume 71 (0471305316) cover image
Consists of 30 checked and edited experimental procedures that illustrate new synthetic techniques or describe the preparation of particularly useful chemicals. Features procedures exemplifying important methods for preparing enantiomerically pure substances by asymmetric catalysis; details a reliable zirconium-based process for the coupling of alkynes and enones; concludes with the preparation of four useful starting materials. A section on waste disposal information is included.
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Partial table of contents:

Asymmetric Hydrogenation of 3-OXO Carboxylates Using Binapruthenium Complexes: (R)-(-)-Methyl 3-Hydroxybutanoate (M. Kitamura, et al.).

Direct Degradation of the Biopolymer Poly [(R)-3-Hydroxybutyric Acid] to (R)-3-Hydroxybutanoic Acid and Its Methyl Ester (D. Seebach, et al.).

3-(S)-[(tert-Butyldiphenylsilyl)-Oxy]-2-Butanone (L. Overman & G. Rishton).

Schwartz's Reagent (S. Buchwald, et al.).

4-Methoxy-4'-Nitrobiphenyl (J. Stille, et al.).

Ubiquinone-1 (Y. Naruta & K. Maruyama).

Benzoannelation of Ketones: 3,4-Cyclododeceno-1-Methylbenzene (M. Tius & G. Kannangara).

2-Methylene-1, 3-Dithiolane (K. Dahnke & L. Paquette).

Methoxycarbonylmethylation of Aldehydes Via Siloxycyclopropanes: Methyl 3,3-Dimethyl-4-Oxobutanoate (H.-U.

Reissig, et al.).

9-Bromo-9-Phenylfluorene (T. Jamison, et al.).

Indexes.
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