 Preparative Chromatography: of Fine Chemicals and Pharmaceutical Agents
ISBN: 978-3-527-30643-5
Hardcover
485 pages
May 2005
US $215.00
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1 Introduction (R. Ditz).
1.1 Liquid Chromatography – its History.
1.2 Focus of the Book.
1.3 How to Read this Book.
2 Fundamentals and General Terminology (M. Schulte, A. Epping).
2.1 Principles of Adsorption Chromatography.
2.2 Basic Effects and Chromatographic Definitions.
2.3 Fluid Dynamics.
2.4 Mass Transfer Phenomena.
2.5 Equilibrium Thermodynamics.
2.6 Thermodynamic Effects on Mass Separation.
2.7 Practical Aspects of Parameter Determination.
3 Columns,Packings and Stationary Phases (K. K. Unger, C. du Fresne von Hohenesche, M. Schulte).
3.1 Column Design.
3.2 Column Packings.
3.3 Column Packing Technology.
3.4 Column Testing.
3.5 Column Maintenance and Regeneration.
3.6 Guidelines for Choosing Chromatographic Columns and Stationary Phases.
4 Selection of Chromatographic Systems (W. Wewers, J. Dingenen, M. Schulte, J. Kinkel).
4.1 Definition of the Task.
4.2 Properties of Chromatographic Systems.
4.3 Criteria for Choice of Chromatographic Systems.
5 ProcessConcepts (M. Schulte, K. Wekenborg, W. Wewers).
5.1 Design and Operation of Equipment.
5.2 Discontinuous Processes.
5.3 Continuous Processes.
5.4 Guidelines.
6 ModelingandDetermination of Model Parameters (M. Michel, A. Epping, A. Jupke).
6.1 Introduction.
6.2 Models for Single Chromatographic Columns.
6.3 Modeling HPLC Plants.
6.4 Numerical methods.
6.5 Parameter Determination.
6.6 Validation of Column Models.
6.7 Modeling of SMB Processes.
7 ModelBasedDesign and Optimization (A. Susanto, K. Wekenborg, A. Epping, A. Jupke).
7.1 Basic Principles.
7.2 Batch chromatography.
7.3 SMB Chromatography.
7.4 Comparison of Batch and SMB Chromatography.
8 Chromatographic Reactors (T. Borren, J. Fricke).
8.1 Introduction.
8.2 Types of Chromatographic Reactors.
8.3 Modeling of Chromatographic Reactors.
8.4 Operation and Design of Chromatographic Reactors.
8.5 Design Examples.
9 AdvancedControl of Simulated Moving Bed Processes (A. Toumi, S. Engell).
9.1 Introduction.
9.2 Model Predictive Control.
9.3 State-of-the-art in Control of SMB Processes.
9.4 Online Optimizing Control of a Reactive Simulated Moving Bed Process.
9.5 Conclusions.
Outlook.
References.
Appendix A.
A1 Scale-up Factors Between Different Columns.
A.2 Standard Operating Procedures for Column Packing.
Appendix B: Data of Test Systems.
B.1 EMD53986.
B.2 Tröger’s Base.
B.3 Glucose and Fructose.
B.4 g -Phenethyl Acetate.
Index.
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