 Basic One- and Two-Dimensional NMR Spectroscopy, 4th, Completely Revised and Updated Edition
ISBN: 978-3-527-31233-7
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430 pages
March 2005
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1.1 Introduction.
1.2 Nuclear Angular Momentum and Magnetic Moment.
1.3 Nuclei in a Static Magnetic Field.
1.4 Basic Principles of the NMR Experiment.
1.5 The Pulsed NMR Method.
1.6 Spectral Parameters: a Brief Survey.
1.7 “Other” Nuclides.
1.8 Bibliography for Chapter 1.
2 The Chemical Shift.
2.1 Introduction.
2.2 1H Chemical Shifts of Organic Compounds.
2.3 13C Chemical Shifts of Organic Compounds.
2.4 Relationships between the Spectrum and the Molecular Structure.
2.5 Chemical Shifts of “Other” Nuclides.
2.6 Bibliography for Chapter 2.
3 IndirectSpin-Spin Coupling.
3.1 Introduction.
3.2 H,H Coupling Constants and Chemical Structure.
3.3 C,H Coupling Constants and Chemical Structure.
3.4 C,C Coupling Constants and Chemical Structure.
3.5 Correlations between C,H and H,H Coupling Constants.
3.6 Coupling Mechanisms.
3.7 Couplings of “Other” Nuclides (Heteronuclear Couplings).
3.8 Bibliography for Chapter 3.
4 Spectrum Analysis and Calculations.
4.1 Introduction.
4.2 Nomenclature.
4.3 Two-Spin Systems.
4.4 Three-Spin Systems.
4.5 Four-Spin Systems.
4.6 Spectrum Simulation and Iteration.
4.7 Analysis of 13C NMR Spectra.
4.8 Bibliography for Chapter 4.
5 Double Resonance Experiments.
5.1 Introduction.
5.2 Spin Decoupling in 1HNMR Spectroscopy.
5.3 Spin Decoupling in 13C NMR Spectroscopy.
5.4 Bibliography for Chapter 5.
6 Assignment of <sup>1</sup>H and <sup>13</sup>C Signals.
6.1 Introduction.
6.2 <sup>1</sup>HNMR Spectroscopy.
6.3 <sup>13</sup>C NMR Spectroscopy.
6.4 Computer-aided Assignment of 13C NMR Spectra.
6.5 Bibliography for Chapter 6.
7 Relaxation.
7.1 Introduction.
7.2 Spin-Lattice Relaxation of <sup>13</sup>C Nuclei (<I>T<sub>1</sub></I>).
7.3 Spin-Spin Relaxation (<I>T<sub>2</sub></I>).
7.4 Bibliography for Chapter 7.
8 One-Dimensional NMR Experiments using Complex Pulse Sequences.
8.1 Introduction.
8.2 Basic Techniques Using Pulse Sequences and Pulsed Field Gradients.
8.3 The J-Modulated Spin-Echo Experiment.
8.4 The Pulsed Gradient Spin-Echo Experiment.
8.5 Signal Enhancement by Polarization Transfer.
8.6 The DEPT Experiment.
8.7 The Selective TOCSY Experiment.
8.8 The One-Dimensional INADEQUATE Experiment.
8.9 Bibliography for Chapter 8.
9 Two-Dimensional NMR Spectroscopy.
9.1 Introduction.
9.2 The Two-Dimensional NMR Experiment.
9.3 Two-Dimensional J-Resolved NMR Spectroscopy.
9.4 Two-Dimensional Correlated NMR Spectroscopy.
9.5 The Two-Dimensional INADEQUATE Experiment.
9.6 Summary of Chapters 8 and 9.
9.7 Bibliography for Chapter 9.
10 The Nuclear Overhauser Effect.
10.1 Introduction.
10.2 Theoretical Background.
10.3 Experimental Aspects.
10.4 Applications.
10.5 Bibliography for Chapter 10.
11 Dynamic NMR Spectroscopy (DNMR).
11.1 Introduction.
11.2 Quantitative Calculations.
11.3 Applications.
11.4 Bibliography for Chapter 11.
12 Shift Reagents.
12.1 Lanthanide Shift Reagents (LSRs).
12.2 Chiral Lanthanide Shift Reagents.
12.3 Chiral Solvents.
12.4 Bibliography for Chapter 12.
13 Macromolecules.
13.1 Introduction.
13.2 Synthetic Polymers.
13.3 Biopolymers.
13.4 Bibliography for Chapter 13.
14 NMR Spectroscopy in Biochemistry and Medicine.
14.1 Introduction.
14.2 Elucidating Reaction Pathways in Biochemistry.
14.3 High-Resolution in vivo NMR Spectroscopy.
14.4 Magnetic Resonance Tomography.
14.5 Bibliography for Chapter 14.
Subject Index.
Index of Compounds.
