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Inorganic Syntheses, Volume 3

Inorganic Syntheses, Volume 3

Ludwig F. Audrieth (Editor-in-Chief)

ISBN: 978-0-470-13234-0

Jan 2007

230 pages

Select type: O-Book


The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Chapter I.

1 Sodium Peroxide 8-Hydrate.

Chapter II.

2 Basic Beryllium Derivatives of Organic Acids.

3 Basic Beryllium Acetate and Propionate.

4 Strontium Sulfide and Selenide Phosphors.

5 Barium Thiocyanate.

Chapter III.

6 Boron Chloride and Bromide.

7 Aluminum Bromide.

Chapter IV.

8 Carbon Tetraiodide.

9 Cyanamide.

10 Dicyanodiamide (Cyanoguanidine).

11 Aminoguanidonium Hydrogen Carbonate (Aminoguanidine Bicarbonate).

12 Ammonium Dithiocarbamate.

13 Organosilicon Compounds.

14 Dimethyldichlorosilane (Dimethylsilicon Dichloride).

15 Vinylchlorosilanes.

16 Diphenylsilanediol.

17 Germanium(II) Iodide (Germanium Diiodide).

18 Methylgermanium Triiodide (Methyltriiodogermane).

19 The Extraction of Hafnium and Zirconium from Cyrtolite.

Chapter V.

20 Nitrogen(V) Oxide (Nitrogen Pentoxide, Dinitrogen Pentoxide, Nitric Anhydride).

21 Hydroxylammonium Salts.

22 The Poly- and Metaphosphates and the Strong Phosphoric Acids.

23 Pyrophosphoric Acid (Diphosphoric Acid).

24 Sodium Pyrophosphates (Sodium Diphosphates).

25 Sodium Triphosphate (Sodium Tripolyphosphate).

26 Sodium Metaphosphates.

27 Sodium Monofluophosphates.

28 Silver Monofluophosphate.

29 Hexafluophosphates of Sodium, Ammonium, and Potassium.

30 Ammonium Metavanadate.

Chapter VI.

31 Sulfur(VI) Fluoride (Sulfur Hexafluoride).

32 Disulfur Pentoxydichloride (Pyrosulfuryl Chloride).

33 Selenium(IV) Oxide (Selenium Dioxide).

34 Selenium(IV) Oxychloride.

35 Crystalline Selenic Acid.

36 Tellurium(IV) Chloride (Tellurium Tetrachloride).

37 Tellurium(IV) Oxide (Tellurium Dioxide).

38 Telluric Acid.

39 Chromium(II) Acetate (Chromous Acetate).

40 Anhydrous Chromium(II) Chloride (Chromous Chloride).

41 Hexaamminechromium(III) Nitrate.

42 Chromium Hexacarbonyl.

43 Potassium Octacyanomolybdate(IV) 2-Hydrate (Potassium Molybdocyanide Dihydrate).

44 Tungsten(VI) Chloride (Tungsten Hexachloride).

45 Uranium(IV) Oxalate.

46 Potassium Tetraoxalatouranate(IV).

Chapter VII.

47 Anhydrous Metal Fluorides.

48 Bromine(III) Fluoride (Bromine Trifluoride).

49 Rhenium(VI) Oxide (Rhenium Trioxide).

50 Rhenium(VII) Oxide (Dirhenium Heptoxide).

Chapter VIII.

51 Anhydrous Iron(III) Chloride (Ferric Chloride).

52 Hexamminenickel(II) Bromide and Hexamminecnickel(II) Iodide.

53 Bis(N,N'-Disalicylalethylenediamine)-μ-Aquodicobalt(II)(Bis[N,N'-bis(o-hydroxybenzylidine)ethylenediamine]-μ-aquodicobalt(II)).

Index of Contributors.

Subject Index.

Formula Index.