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Inorganic Syntheses, Volume 4



Inorganic Syntheses, Volume 4

John C. Bilar Jr. (Editor-in-Chief)

ISBN: 978-0-470-13267-8 September 2009 265 Pages

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The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Chapter IA.

1 Lithium Nitride.

2 Extraction of Cesium from Pollucite.

Chapter IB.

3 Silver(II) Oxide.

4 Gold Powder and Potassium Tetrabromoaurate(III).

Chapter IIA.

5 Calcium Dihydrogen Orthophosphate 1-Hydrate.

6 Calcium Hydrogen Orthophosphate 2-Hydrate and Calcium Hydrogen Orthophosphate.

Chapter IIIA.

7 Aluminum Phosphide.

Chapter IV.

8 Biurea.

9 Urazine.

10 Carbohydrazide.

11 Cyanate Condensation Products of Carbohydrazide.

12 Thiosemicarbazide.

13 Iodotrichlorosilane and Diiododichlorosilane.

14 Cyclohexyltrichlorosilane.

15 Silicon Tetraacetate.

Chapter V.

16 Nitrosyl Chloride.

17 Nitryl Chloride.

18 Phosphorous Acid.

19 Diethyl Phosphite.

20 Dioctyl Phosphite.

21 Alkyl Dichlorophosphites.

22 2-Chloroethyl Dichlorophosphite.

23 Disodium Dihydrogen Hypophosphate.

24 Phosphorus(V) Sulfochloride.

25 O-Ethyl Dichlorothiophosphate.

26 Diethyl Monoamidophosphate.

27 Diethyl Monochlorophosphate.

28 Vanadium(III) Oxide and Vanadium(V) Oxytrichloride (Correction).

Chapter VIA.

29 Sodium Superoxide.

30 2-Chloroethyl Chlorosulfonate and (2-Chloroethoxy)-trichlorosilane.

31 Sodium “Selenopentathionate” 3-Hydrate and Sodium “Telluropentathionate” 2-Hydrate.

32 Xanthates and Dithiocarbamates of Selenium(II) and Tellurium(II).

Chapter VIB.

33 Addition Compounds of Chromium(VI) Oxide.

34 Potassium Pentachloroaquomolybdate(III) and Potassium hexachloromolybdate(III).

35 Bis(8-quinolinolo)dioxouranium(VI) and Its Addition Compound with 8-Quinolinol.

Chapter VIIA.

36 Anhydrous Metal Halides.

37 Gallium (II) Chloride.

38 Bismuth(III) Iodide.

39 Aluminum Iodide.

40 Tin(IV) Iodide.

41 Zirconium and Hafnium Tetrachlorides.

42 Vanadium(II) Chloride.

43 Vanadium(III) Chloride.

44 Tantalum(V) Bromide.

45 Fluorination of Volatile Compounds.

46 Methyl Chlorofluorophoshpite and Methyl Difluorophosphite.

47 Silicon Tetrafluoride.

48 Germanium(IV) Fluoride.

49 Phosphorus(III) Fluoride.

50 Arsenic(III) Fluoride.

51 Chlorine(IV) Oxide.

Chapter VIII.

52 Iron(II) Formate.

53 Iron(II) Bromide 6-Ammoniate.

54 Potassium Ferrate(VI).

55 Nitrosylpentamminecobalt(II) Chloride, Black and Nitrosylpentamminecobalt(III) Chloride, Pink.

56 Acidopentamminecobalt(III) Salts.

57 cis- and trans-Dinitrobis(ethylenediamine)cobalt(III) Nitrate.

58 trans-Dinitrodiamminepalladium(II).

Index of Contributors.

Subject Index.

Formula Index.