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Inorganic Syntheses, Volume 5

Inorganic Syntheses, Volume 5

Therald Moeller (Editor-in-Chief)

ISBN: 978-0-470-13236-4 January 2007 216 Pages

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The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Chapter IA.

1 Lithium Hydroperoxide 1-Hydrate, Lithium Peroxide and Lithium Oxide.

2 Sodium Dispersions.

3 Sodium Hydride.

Chapter IB.

4 Dichloro(di-2-pyridylamine)copper(II) and Bis(di-2-pyridylamine)copper(II).

5 Bis(ethylenediamine)copper(II) Diiodocuprate(I).

6 Disilver Fluoride.

Chapter IIA.

7 Beryllium Chloride.

Chapter IIIA.

8 Boron Halide-Amine Coordination Compounds.

9 Ethyl Orthoborate.

Chapter IIIB.

10 Isolation of Samarium, Europium, and Ytterbium Materials by Means of Sodium Amalgam.

11 Anhydrous Lanthanon Nitrates.

Chapter IVA.

12 Cyanogen.

13 Allophanyl Hydrazide.

14 Urazole.

15 Silica Gel (Correction).

16 Organosilazane Compounds.

17 Organogermanium Compounds.

18 Tetraphenylgermane.

19 Hexaphenyldigermane.

20 Diphenylgermane.

21 Triphenylbromogermane and Triphenylgermane.

Chapter IVB.

22 Extraction of Titanium(IV) Oxide from Ilmenite.

23 Titanium(IV) Sulfide.

Chapter VA.

24 Nitrogen(IV) Oxide.

25 1,1,1-Trisubstituted Hydrazonium Chlorides.

26 Phosphorus(III) Fluoride.

27 Hexaguanidonium Tetraphosphate 1-Hydrate.

28 Sodium Monothiophosphate.

Chapter VB.

29 Preparation of Metal Derivatives of 1,3-Diketones.

30 Vanadium(IV) Oxy(acetylacetonate).

Chapter VIA.

31 N-Nitrosohydroxylamine-N-sulfonates.

32 Hydroxylamine-O-sulfonic Acid.

33 Selenium(IV) Chloride.

Chapter VIB.

34 Chromium(III) Iodide.

35 Chromium(III) Acetylacetonate.

36 Aquopentammine- and Acidopentamminechromium(III) Salts.

37 Tungsten Hexacarbonyl.

38 Tripotassium Enneachloroditungstate(III).

39 Uranium(IV) Chloride.

40 Uranium(III) Chloride.

41 Uranyl Chloride.

42 Uranyl Hydrogen Orthophosphate 4-Hydrate.

Chapter VIIA.

43 Anhydrous Metal Chlorides.

44 Chlorine(I) Compounds.

45 Purifaction of “Carrier-free” Iodine-131 Activity.

46 Polyhalogen Complex Salts.

47 Typical Polyhalogen Salts.

Chapter VIII.

48 Iron(II) Chloride 2-Hydrate.

49 Cobalt(III) Sulfate 18-Hydrate.

50 Dichloro(di-2-pyridylamine)cobalt(II).

51 Nitrosylpentamminecobalt(II) Chloride, Black, and Nitrosylpentamminecobalt(III) Chloride, Pink (Correction).

52 Barium(Ehtylenediaminetetraacetato)cobaltate(III) 4-Hydrate.

53 Cobalt(III) Acetylacetonate.

54 Dicobalt Octacarbonyl.

55 Cobalt Tetracarbonyl Hydride.

56 Nickel Powder.

57 Potassium Hexacyanodinickelate(I).

58 Sodium and Potassium Nickel(IV) Paraperiodates.

59 Ammonium Hexabromoosmate(IV).

60 Ammoniuim Hexachloroosmate(IV).

61 Platinum(II) Chloride.

62 Tetrachloro(diethylene)diplatinum.

Index of Contributors.

Subject Index.

Formula Index.