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Inorganic Syntheses, Volume 7



Inorganic Syntheses, Volume 7

Jacob Kleinberg (Editor-in-Chief)

ISBN: 978-0-470-13270-8 September 2009 335 Pages

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The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Chapter IA.

1 Lithium Hydroxide and Lithium Oxide.

Chapter IB.

2 1-Phenylbiguanide-p-sulfonic Acid Complexes of Copper(II).

3 Tetrakis[iodo(tri-n-butylphosphine)copper(I)] and Iodo-(2,2'-bipyridine)(tri-n-butylphosphine)copper(I).

Chapter IIA.

4 Barium Iodate 1-Hydrate.

Chapter IIIA.

5 Gallium(III) Nitride.

6 Indium(I) Bromide.

Chapter IVA.

7 Hexachlorodisiloxane.

8 Trichlorosilanethiol.

9 Tris(acetylacetonato)silicon Chloride Hydrochloride and Some Derivatives.

10 Hydrides of Germanium, Tin, Arsenic, and Antimony.

Chapter IVB.

11 Titanium(III) Chloride.

12 Bis[tris(acetylacetonato)titanium(IV)] Hexachlorotitanate(IV).

13 Zirconium(IV) Iodide.

Chapter VA.

14 Biguanide Sulfate.

15 Biguanide.

16 Black Phosphorus.

17 Pentacalcium Monohydroxyorthophosphate.

18 Tetrammonium Pyrophosphate.

19 (Triphenyl)aminophosphonium Chloride.

20 (Dimethylamido)phosphoryl Dichloride.

21 Bis(dimethylamido)phosphoryl Chloride.

22 Octamethylpyrophosphoramide.

23 Trimeric and Tetrameric Phosphonitrile Bromides.

24 Phosphorus(V) Chloride–Boron Chloride Complex.

25 Phosphorus(V) Chloride–Gallium(III) Chloride Complex.

26 Methylbromoarsines.

Chapter VB.

27 Vanadium(III) Fluoride.

28 Vanadium(III) Sulfate.

29 Vanadium(II) Sulfate.

30 Vanadium(II) Hydroxide.

31 Cyclopentadienyl Metal Carbonyls and Some Derivatives.

Chapter VIA.

32 Sulfur(S35).

33 Sulfur(IV) Fluoride.

34 Peroxydisulfuryl Difluoride.

35 Sodium Hydrogen Sulfide.

Chapter VIB.

36 Trichloro(tripyridine)chromium(III).

37 Tris(3-bromoacetylacetonato)chromium(III).

38 Cyclopentadienyl Tricarbonyl Hydrides of Chromium, Molybdenum, and Tungsten.

39 Trichloro(tripyridine)molybdenum(III).

40 Potassium Octacyanotungstate(IV) 2-Hydrate.

41 Uranyl Chloride 1-Hydrate.

Chapter VIIA.

42 Sodium Fluoride(F18).

43 Chlorine(Cl36)-Labeled Deuterium Chloride.

44 Chlorine(Cl36)-Labeled Thionyl Chloride, Silicon Tetrachloride, Boron Chloride, Germanium(IV) Chloride and Phosphorus(III) Chloride.

45 Anhydrous Metal Chlorides.

46 Unipositive Halogen Complexes.

47 Monopyridineiodine(I) Chloride.

48 Anhydrous Hydrogen Iodide.

Chapter VIIB.

49 Acetylacetonato manganese(III).

50 Rhenium(III) Iodide.

51 Potassium Hexachlororhenate(IV) and Potassium Hexabromorhenate(IV).

Chapter VIII.

52 Triiron Dodecacarbonyl.

53 Sodium Salts of Carbonyl Hydrides Prepared in Ethereal Media.

54 Iron-labeled Cyclopentadienyl Iron Complexes.

55 Tris(3-nitroacetylacetonato)cobalt(III).

56 Inner Complexes of Cobalt(III) with Diethylenetriamine.

57 Hydrated Rhodium(III) Chloride, Chloroamminerhodium(III) Salts, and a Note on the Recovery of Rhodium Wastes.

58 cis- and trans-Tetrachloro(dipyridine)iridium(IV).

59 cis- and trans-Trichloro(diethyl sulfide)iridium(III).

60 cis- and trans-Pyridium Tetrachloro(dipyridine)iridate(III).

61 Recovery of Platinum from Laboratory Residues.

62 cis- and trans-Tetrachlorodiammineplatinum(IV).

63 cis- and trans-Dichlorodiammineplatinum(II).

64 cis- and trans-Dichlorobis(tri-n-butylphosphine)platinum(II).

65 cis- and trans-Dichloro(dipyridine)platinum(II).

Index of Contributors.

Subject Index.

Formula Index.