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Inorganic Syntheses, Volume 9



Inorganic Syntheses, Volume 9

S. Young Tyree Jr. (Editor-in-Chief)

ISBN: 978-0-470-13275-3 September 2009 241 Pages

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The volumes in this continuing series provide a compilation of current techniques and ideas in inorganic synthetic chemistry. Includes inorganic polymer syntheses and preparation of important inorganic solids, syntheses used in the development of pharmacologically active inorganic compounds, small-molecule coordination complexes, and related compounds. Also contains valuable information on transition organometallic compounds including species with metal-metal cluster molecules. All syntheses presented here have been tested.

Notice to Contributors.

Chapter I.

Cross-listing of Group I Compounds in other chapters.

Chapter II.

1 Dichlorobis(hydroxylamine)zinc(II).

Chapter III.

2 Diamminedihydroboron(1+) tetrahydroborate.

3 Trimethylamine-borane, (Dimethylamino)borane, and N, N', N''-trimethylborazine.

4 Hydrazine-mono- and -bisborane.

5 Bis(triethylammonium decahydrodecaborate(2–).

6 Diphenylphosphine and Dimeric (Diphenylphosphino)boranes.

7 Aluminum derivative of Ethyl Acetoacetate.

8 Tris(1,1,1,5,5,5-hexafluoro-2,4-pentanedionato)aluminum.

9 Trimethylamine-aluminum hydride and Trimethylamine-aluminum chloride dihydride.

10 Tris(1-phenyl-1,3-butanedionato)europium(III) 2-hydrate.

11 Uranium(IV) acetate.

Chapter IV.

12 Hexaureatitaniuim(III) percholate.

13 Titanium(IV) bromide.

14 Tetrakis(1,1,1-trifluoro-2,4-pentanedionato)zirconium(and hafnium).

15 Diphenylbis(1-phenyl-1,3-butanedionato)tin(IV).

Chapter V.

16 Phosphine.

17 Trimethylphosphine.

18 Fluorophosphoranes.

19 Phenyldibromophosphine.

20 Phosphonitrile fluorides.

21 Vanadium(V) oxide.

22 Vanadium(V) oxide and Chromium(VI) oxide nitrate.

23 Niobium(V) chloride and Hexachloroniobates(V).

24 Trimethylantimony dihalides.

Chapter VI.

25 Tetrasulfur tetranitride, S4N4.

26 Sulfur nitrogen chlorides.

27 Sulfuryl chloride fluoride and Sulfuryl fluoride.

28 Potassium fluorosulfite.

29 Cobalt(II) sulfoxylate.

30 Bis(triarylphosphoranylidene)sulfamides and N,N-dialykyl-N'-(triarylphosphoranylidene)sulfamides.

31 Cycloheptatrienemolybdenum(0) tricarbonyl.

32 Tungsten oxide and tetrachloride.

Chapter VII.

33 Chlorine(I) nitrate.

34 Iodine(I) chloride.

35 Anhydrous metal chlorides: Vanadium(III) chloride, Niobium(V) chloride, Molybdenum(V) chloride, and Tungsten(VI) chloride.

36 Tetrahalo complexes of dipositive metals in the first transition series.

37 Triorthoperiodatotetracobaltic(III) acid.

38 Complexes of rhenium(V).

39 Trimethylsilyl perrhenate.

Chapter VIII.

40 Metal iron(III) oxides.

41 Hexaamminecobalt(II) chloride.

42 Chloropentaamminecobalt(II) chloride.

43 cis-Bromochlorobis(ethylenediamine)cobalt(III) bromide 1-hydrate and trans-Bromochlorobis(ethylenediamine)-cobalt(III) nitrate.

44 2,4-Pentanedionatobis(ethylenediamine)cobalt(III) ion.

45 Potassium tetranitrodiamminecobaltate(III).

46 Salts of dinitrodiglycinatocobaltate.

47 Bromo(tetraethylenepentamine)cobalt(III) bromide.

48 Perchloratonickel(III) complexes.

49 Tetrakis(triphenyl phosphite)nickel(0).

50 Ammonium hexachloroplatinate(IV).


Index of Contributors.

Subject Index.

Formula Index.