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Organic Syntheses, Volume 77

Organic Syntheses, Volume 77

David J. Hart (Editor)

ISBN: 978-0-471-39567-6

Sep 2000

352 pages

Select type: Hardcover

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Organic Syntheses, Volume 77 describes twenty-eight checked and edited experimental procedures, spanning a broad range of synthetic methodologies, and provides chemists with a compendium of new or little known experimental procedures which lead to useful compounds or that illustrate important new developments in methodology. For every procedure, safety warnings are presented along with detailed descriptions for the preparation, purification, and identification of the compound in question. Additionally, special reaction conditions are detailed, along with the source of reagents, helpful waste disposal guidelines, discussions of results, references to the primary literature, and an appendix of nomenclature and registry numbers. Coverage is divided into four main sections devoted to: reagents and procedures for asymmetric synthesis; chemical processes; chemical reagents; and chemical compounds, respectively.

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Partial table of contents:Preparation of (R,R)-1,2:4,5-Diepoxypentane (S. Rychnovsky, et al.).

Synthesis and Diastereoselective Alkylation of Pseudoephedrine Amides (A. Myers & B. Yang).

(R)-(+)-2-Hydroxy-1,2,2-Triphenylethyl Acetate (J. Macor, et al.).

Synthesis of 1,1-Dimethylethyl (S)-4-Formyl-2,2-Dimethyl-3-Oxazolidinecarboxylate By Reduction of the Alcohol (A. Dondoni & D. Perrone).

Synthesis of (S,E)-1-(Methoxymethoxy)-1-Tributylstannyl-2-Butene (J. Marshall, et al.).

Allylindation in Aqueous Media: Methyl 3-(Hydroxymethyl)-4-Methyl-2-Methylenepentanoate (G. Bennett & L. Paquette).

The Synthesis of 2-Alkyl-4-Pyrones From Meldrum's Acid (M. Crimmins, et al.).

9-Ethyl-3,6-Dimethylcarbazole (DMECZ) (J. Buck, et al.).

Bis(Pinacolato)Diboron (T. Ishiyama, et al.).

-Tosylbenzyl Isocyanide (J. Sisko, et al.).

Methyl 2,3-O-(6,6'-Octahydro-6,6'-Bi-2H-Pyran-2,2'-Diyl)--D-Galactopyranoside (S. Ley & H. Osborn).

Cyclopropylacetylene (E. Corley, et al.).

3-Nitropropanal, 3-Nitropropanol, and 3-Nitropropanal Dimethyl Acetal (H. Griesser, et al.).

Cyclopropene: A New Synthesis and Its Diels-Alder Reaction with Cyclopentadiene (P. Binger, et al.).

Unchecked Procedures.